浩瀚色譜（山東）應用技術開發有限公司,是齊魯大地一家從事色譜儀器技術開發，技術推廣的技術型企業，研發出多款新型產品。（一）專用色譜柱：1.氯乙suan直接進樣分析專用柱2.氯化氫直接進樣分析專用柱3.氯QI直接進樣分析專用柱4.四氟化硅直接進樣分析專用柱5.六氟二甲基硅醚分析專用柱6.氨氣直接進樣分析專用柱（二）痕量分析專用氣相色譜儀：1.高純氣體中痕量水（ppb級）分析專用氣相色譜儀2.純苯中痕量噻吩（ppb級）分析專用氣相色譜儀（三）防腐型氣相色譜儀，并成功應用于氟氣，氟化氫，氯QI，氨氣，酰氯，氯化氫，三氯氫硅，四氟化硅，氯YI酸，氯HUA亞砜，硫化物，二氯化硫等腐蝕性物質檢測，產品遍布各個行業及地區，其中不乏有大型央企---中石油，中儲糧，秦山核電站，中紡集團等，部分出口。

公司主要業務

1.通用氣相色譜儀生產銷售：氫火焰檢測器氣相色譜儀，熱導檢測器氣相色譜儀，火焰光度檢測器氣相色譜儀，氮磷檢測器氣相色譜儀，電子捕獲檢測器氣相色譜儀。

2.便攜式氣相色譜儀，在線氣相色譜儀生產銷售。

3.專用氣相色譜儀研發制造：氧化鋯檢測器氣相色譜儀，氦離子檢測器氣相色譜儀，氬離子檢測器氣相色譜儀等。

4.防腐氣相色譜儀

5.二維，多維氣相色譜儀

6.高效液相色譜儀

7.實驗室純水機，頂空進樣器，自動進樣器，熱解析儀，氮氫空發生器，色譜耗材（色譜柱，石墨墊，穩壓閥，壓蓋鉗，頂空瓶，7725進樣閥等），分光光度計，電子天平，水分測定儀，干燥箱，離心機，玻璃儀器，化學試劑等整套實驗室設備生產銷售。

8.提供技術轉讓，建立分析方法。

9.從事舊色譜以舊換新的業務。

10.色譜柱研制，定做。

11.承接樣品的檢測業務。

12.承接國內外色譜儀器的維修，改裝業務。

浩瀚色譜（山東）應用技術開發有限公司，以客戶為中心，想客戶所想，銷售的不僅僅是產品，重要的是幫助客戶解決問題，架起心靈溝通的橋梁。

固定液：6%氰丙基苯基-94%甲基聚硅氧烷

極性： 中等極性

使用溫度：40℃～240℃

規格：30m*0.53mm*3um

型號：HH-624

應用：中國藥典2015 二部 乙醇量測定

法（毛細管柱法）
色譜條件與系統適用性試驗  采用（6%）氰丙基苯基-（94%）二甲基聚硅氧烷為固定液的毛細管柱；起始溫度為40℃，維持2分鐘，以每分鐘3℃的速率升溫65℃，再以每分鐘25℃的速率升溫200℃，維持10分鐘；進樣口溫度200℃；檢測器（FID）溫度220℃；采用頂空分流進樣，分流比為1：1；頂空瓶平衡溫度為85℃，平衡時間為20分鐘。理論板數按乙醇峰計算應不低于10000，乙醇峰與正丙醇峰的分離度應大于2.0。
校正因子測定 精密量取恒溫20℃的無水乙醇5ml，平行兩份；置100ml量瓶中，精密加入恒溫20℃的正丙醇（內標物質）5ml，用水稀釋刻度，搖勻，精密量取該溶液1ml，置100ml量瓶中，用水稀釋刻度，搖勻（必要時可進一步稀釋），作為對照品溶液。精密量取3ml，置10ml頂空進樣瓶中，密封，頂空進樣，每份對照品溶液進樣3次，測定峰面積，計算平均校正因子，所得校正因子的相對標準偏差不得大于2.0%。
測定法 精密量取恒溫20℃的供試品適量（相當于乙醇約5ml），置100ml量瓶中，精密加入恒溫20℃的正丙醇5ml，用水稀釋刻度，搖勻，精密量取該溶液1ml，置100ml量瓶中，用水稀釋刻度，搖勻（必要時可進一步稀釋），作為供試品溶液。精密量取3ml，置10ml頂空進樣瓶中，密封，頂空進樣，測定峰面積，按內標法以峰面積計算，即得。
【附注】毛細管柱建議選擇大口徑、厚液膜色譜柱，規格為30m×0.53mm×3.00μm。


中國藥典2015 二部 乙醇量測定 測試譜圖：


Chinese Pharmacopoeia 2015 Part Two Determination of Ethanol Amount
Chinese Pharmacopoeia 2015 Part Two Detailed information on determination of ethanol content:


Name: Capillary Column
Fixing fluid: 6% cyanopropyl phenyl-94% methyl polysiloxane

Polarity: medium polarity

Operating temperature: 40℃～240℃

Specification: 30m*0.53mm*3um

Model: HH-624

Application: 2015 Chinese Pharmacopoeia Part II Determination of ethanol content

The first method (capillary column method)
The chromatographic conditions and system suitability test use (6%) cyanopropyl phenyl-(94%) dimethyl polysiloxane as the fixed liquid capillary column; the starting temperature is 40 ℃, maintained for 2 minutes, every minute The temperature is increased to 65°C at a rate of 3°C, and then to 200°C at a rate of 25°C per minute, and maintained for 10 minutes; the temperature of the injection port is 200°C; the temperature of the detector (FID) is 220°C; headspace split sampling is used, split flow The ratio is 1:1; the equilibrium temperature of the headspace bottle is 85℃, and the equilibrium time is 20 minutes. The number of theoretical plates should not be less than 10,000 calculated based on the ethanol peak, and the separation between the ethanol peak and the n-propanol peak should be greater than 2.0.
Correction factor determination. Precisely measure 5ml of absolute ethanol at a constant temperature of 20°C, in parallel; place in a 100ml measuring flask, precisely add 5ml of n-propanol (internal standard substance) at a constant temperature of 20°C, dilute to the mark with water, and shake well , Accurately measure 1ml of the solution, put it in a 100ml measuring flask, dilute to the mark with water, shake it up (if necessary, further dilute), as a reference solution. Accurately measure 3ml, place it in a 10ml headspace sampling bottle, seal, and inject headspace, each reference solution is injected 3 times, the peak area is measured, and the average correction factor is calculated. The relative standard deviation of the obtained correction factor shall not be greater than 2.0 %.
Assay method Precisely measure an appropriate amount of the test product (equivalent to about 5ml of ethanol) at a constant temperature of 20°C, place it in a 100ml measuring flask, and add 5ml of n-propanol at a constant temperature of 20°C, dilute to the mark with water, shake well, and measure accurately Take 1ml of the solution, put it in a 100ml measuring flask, dilute to the mark with water, shake it up (if necessary, further dilute), as the test solution. Accurately measure 3ml, place it in a 10ml headspace sample bottle, seal it, inject the sample in the headspace, measure the peak area, and calculate the peak area according to the internal standard method.
[Note] The capillary column is recommended to choose a large-diameter, thick liquid film chromatography column, the specification is 30m×0.53mm×3.00μm.


Chinese Pharmacopoeia 2015 Part Two Determination of the amount of ethanol Test spectrum: