自動微量傾濁點測試儀

MPC-602/302

New Standard ASTM D6749

No Methanol

新標準ASTM D6749，無甲醛

Model MPC-602/302 has been designed for automatic determination of Pour Point (PP) and Cloud Point (CP) with small specimen size and shorter test time while securing better test precision than the conventional manual method’s. PP measurement is made by utilizing a new automatic method, namely Air Pressure method, which yields eventually no bias against the conventional test method’s, repeatability of 1 ℃, and reproducibility of 2 ℃.(*) This epoch-making accuracy has made PP determination at 1 ℃ intervals make more sense. The CP/PP mode executes a CP determination and then a PP determination consecutively, which further improves the test throughput. MPC-602 is a 6 tests version, and MPC-302 is a 3 tests version of its original single test model (MPC-102L). ASTM has approved the PP test method: ASTM D6749 on “Standard Test Method for Pour Point of Petroleum Products (Automatic Air Pressure Method)”. *Accuracy information is for typical samples.

MPC-102系列自動微量傾濁點測試儀，采用微量法測試樣品的傾點，取樣量少，測定過程由計算機自動完成，無需人工干預(yù)，測定速度快而結(jié)果準確。測定樣品的同時可同時測定樣品的濁點。儀器進行傾點測試時，沒有采用傳統(tǒng)的“傾斜法”，而采用了新的標準ASTM D6749 “空氣加壓法”。測試結(jié)果與ISO3016和ASTM D97是所描述的傾斜法完全一致。樣品的測試間隔為1℃/2℃，并同時連續(xù)測試2-3次，測試結(jié)果具有更好的重復(fù)性和再現(xiàn)性。

MPC系列有多種型號可選擇。MPC-302適用于3樣品同時測試，MPC-602用于6樣品同時測試。MPC-102L是液冷型，MPC-102A是風(fēng)冷型。

POUR POINT AT 1 ℃ INTERVALS FOR HIGHER YIELD IN PROCESS:

The conventional PP test methods yield a rough PP numbers of multiple of 3 ℃, and thus higher resolution in PP determination has been long awaited for more elaborate process control. With the patented Air Pressure method, PP can be now determined at 1 ℃ intervals with high accuracy, since the disturbance on the formation of wax crystal structure through the test process is at a minimal level. When PP is measured at 1 ℃ intervals, typical repeatability and reproducibility are 1 ℃ and 2 ℃, respectively.

傳統(tǒng)的“傾斜法”是按3℃間隔測試樣品的傾點，新的標準按1℃間隔測試樣品，儀器測試精度大于試驗標準測試規(guī)定,可以保證試驗結(jié)果的精度更高。“氣壓法”也可有效避免降溫過程中，樣品的蠟狀析出和冰晶體對結(jié)果的干擾。

EASY SAMPLE HANDLING: 采樣少，易操作

Since the required specimen volume is a mere 4.5 ml and the specimen cup is a test-tube type removable jar, the sample handling is extremely easy. 樣品僅需求4.5毫升，玻璃小型樣品杯是一個可取放的瓶狀試管，操作極其簡單。

EASY, QUICK, AND PRECISE PP/CP DETERMINATION:

Just set up the specimen, set test parameters, and then press the START key to start a test. Specimen is cooled at the steepest possible rate without affecting the formation/growth of wax crystal, which has been known to be critical in PP/CP determination. For fuel oils, the specimen may be even pre-heated automatically and then cooled for CP/PP determination, which further improves test throughput.

選好樣品后，輸入測試參數(shù)，預(yù)期的傾/濁點數(shù)據(jù)，按下“開始”鍵。測定過程由儀器自動完成，無需人工干預(yù)。當?shù)綑z測出傾點后，樣品被自動加熱至與室溫一致。從而可在短時間內(nèi)進行多組測試。

相較于傳統(tǒng)測試方式，“氣壓法”的效率更高，一般只要傳統(tǒng)方式的1/3 或 1/2的時間，就可以完成測試。可在短時間內(nèi)進行多組測試。

TANAKA Mini Pour/Cloud Point Tester, series MPC-602/302

SPECIFICATIONS:

TYPE:

Mini Pour Point(PP) and Cloud Point(CP) tester with 6 test heads (MPC-602) or 3 test heads (MPC-302) in Bench-top package.With sequential CP and PP measurement capability. Sample cooling and pre-heating by Peltier modules with external cooling liquid. 應(yīng)用“氣壓法”測試樣品傾點(PP)，濁點(CP)，或樣品的濁點(CP)+傾點(PP)的連續(xù)測定，特有的半導(dǎo)體制冷/加熱設(shè)計，MPC-302適用于3樣品同時測試，MPC-602用于6樣品同時測試。

TEST STANDARDS: 適用標準

ASTM D6749/D97, ISO 3016(PP) , （傾點）

ASTM D2500, ISO 3015 (CP) （濁點）

SPECIMEN VOLUME（樣品量）: 4.5ml

MEASURING RANGE: (typical*)測試范圍

+51 ℃ to -65 ℃ with cooling liquid of -35 ℃ （外接循環(huán)制冷源，介質(zhì)溫度約在零下35℃）

+51 ℃ to -60 ℃ with cooling liquid of -25 ℃ （外接循環(huán)制冷源，介質(zhì)溫度約在零下25℃）

+51 ℃ to -40 ℃ with tap water of 20 ℃ （直接外接循環(huán)水冷，水溫約在20℃）

*:Sample viscosity, etc. affects on lowest temperature of the measuring range.

樣品本身的低溫運動粘度的性質(zhì)，限制了試驗所需要zui低的測試溫度。

MEASUREMENT MODES: 測試模式

Selectable from various modes. 可選擇多種測試模式

1.CP mode濁點測試模式（每隔0.1 或 1.0℃測試）

2.PP modes: Programmed by the user. Programmable 傾點測試模式，按用戶要求組合

parameters are: 需要先選擇油品種類，再選擇測試溫度。

*Amount of applied air pressure for PP detection, to accommodate different sample types: L(low) for diesel fuels, H(high) for lube oils, VH(very high) and UH (ultra high) for residual fuels and similar samples. 按油品種類（L-柴油；H-潤滑油；VH或 UH-重油/渣油）

*Testing intervals: 1.0℃, 2.5℃, or 3.0℃ 按溫度每隔1.0℃, 2.5℃, 或 3.0℃測試

(In total, 4x3=12 modes for PP.) 以上總計12種組合傾點測試模式

3.CP/PP modes: 濁點+傾點連續(xù)測試 （重復(fù)測試）

CP is determined and then PP. PP detection is programmable by the user with the same parameters as PP modes’. (12 modes in total.)

到檢測出傾點后，樣品被自動加熱至與室溫一致，再次連續(xù)測試樣品，或再次按不同的模式測試樣品，尤其適用于科研場合。

SAMPLE AUTOMATIC PRE-HEATING: 樣品自動加熱

Automatic preheating at either +45 ℃ or EPP+10 ℃. (EPP=Expected Pour Point)

按試驗方法對樣品預(yù)熱步驟的要求，儀器也包括了樣品預(yù)熱的功能。每次測試時，樣品會按要求被預(yù)熱到（45℃）或（預(yù)期傾點+10℃）

DISPLAY: （顯示）

Test parameters, EPP, bath temperature, sample temperature, PP, and CP displayed on VFD. Temperatures displayed with 0.1 ℃ increments. VFD熒光屏，清晰顯示試驗參數(shù)，冷浴溫度，樣品溫度，傾點，濁點，預(yù)期傾點等內(nèi)容。

溫度顯示精度0.1℃。

PRINTER: 打印機

(built-in) PP, CP, mode, EPP, etc. printed by thermal printer. 內(nèi)置熱敏式打印機，打印試驗結(jié)果。

EPP SETTING: 預(yù)期傾點設(shè)定

EPP(Expected Pour Point) needs to be set prior to test starts. 測試開始時需要輸入預(yù)期傾點

SPECIMEN CUP: （樣品杯）

Cylindrical glass test jar with 4.5ml sample volume.

石英玻璃的小型樣品杯，每次試驗只需要4.5ml的樣品

SENSORS: 傳感器

Compound type sensor assembly for PP and CP. 同一儀器既可以檢測傾點，也可以檢測濁點

PP detected by air pressure method (patented). （的）氣壓傳感器變化檢測傾點

CP detected photo-electrically. 光電傳感器檢測濁點

PT100 temp. sensors. 鉑電阻檢測溫度

SAMPLE COOLING RATE: 降溫速率

As standard, 4 ℃/min. till EPP+40 ℃, and 1 ℃/min. thereafter. Cooling process is programmable.

按標準規(guī)定：在預(yù)期傾點+40℃以前，降溫速率4℃/min；在此以后，降溫速率1℃/min。

用戶也可以自行設(shè)定特殊的降溫曲線，便于科研應(yīng)用。

SAFETY SHUTDOWN: 安全保護

As hot side of Peltier module reaches 60 ℃ while preheating, warning buzzer beeps and heating stops. 半導(dǎo)體熱面溫度達到（60℃），超過限定時 ，儀器報警提示，并且自動停機

DATA OUTPUT: 數(shù)據(jù)輸出

RS-232C 1 channel標準RS-232C接口，1

POWER REQUIREMENTS: （電源需求）

100, 120, 220,  or 240VAC

1.5kW (MPC-602), 1.0kW (MPC-302)

DIMENSIONS AND WEIGHT: （體積和重量）

800Wx550Dx850H, 100kg (MPC-602)

800Wx500Dx800H,    75kg (MPC-302)

ORDERING INFORMATION:

STANDARD ACCESSORIES: （標準附件）

OPTIONAL ACCESSORIES:       （選購件1）

Water Regulator with Pressure Gauge(for Connecting Tap Water)

循環(huán)泵組件 (直接外接水冷專用)

Chillers for -60 ℃ of Measurement: TANAKA TCU-40B, Neslab RTE-740(*1) or Julabo FP-40MC(*2) Use above chiller x 3 sets for MPC-602, 2 sets for MPC-302

試驗溫度要求-60℃（零下60℃）需要外接循環(huán)制冷源，

MPC-602必須外接3臺制冷源；MPC-302必須外接2臺制冷源

推薦以下型號：

TANAKA TCU-40B（日本田中制）或RTE-740（美國制）或Julabo FP40-MC（德國制）

Chiller for -40 ℃ of Measurement: Use above chiller x 1 set (MPC-602 and 302)

試驗溫度要求-40℃（零下40℃），MPC-602/302必須外接至少1臺循環(huán)制冷源

*1: Made in USA. *2: Made in Germany.

SUGGESTED SPARES FOR 2 YEARS: （選購件2，2年維護）